Optical
Studies Facilities:
The optical laboratory of
nanostructure material and devices laboratory (NMDL)
covers instrumentations enabling a variety of spectroscopic
and microscopic characterizations including: photoluminescence
(PL) spectroscopy, Fourier Transform Infrared (FTIR)
Spectroscopy, cathodoluminescence (CL) spectroscopy,
spectroscopic ellipsometry, and optical microscopy etc.
Two separate home-designed
PL stations currently are in operation. A cw PL (figure
1) station is capable of performing conventional cw
PL and PL excitation (PLE) spectroscopy on both solid
and solution samples at room or cryogenic temperature
(down to 2K). It covers the visible and NIR wavelength
region with a number of excitation sources (ion laser,
Ti:S laser, lamp source etc.) and detectors (GaAs photomultiplier
tube and Ge detector etc). Raman studies are also possible
on this cw PL setup because of its one meter double
monochromator with high stray light rejection. For the
last 10 years this PL setup has been the main work-horse
for optical characterization of the self-assembled
epitaxial nanostructure. Being home-designed other
than standard PL and PLE, this setup is so flexible
that it has been adapted for many other measurements
such as absorption, photocurrent, and electroluminescence
etc whenever research needs.
A second PL (figure 2, 3)
station is designed for more advanced studies especially
on our current work of integrated
epitaxial and colloidal nanostructure. Other the
standard cw PL and cryogenic capability, it can also
perform time resolved PL (TRPL) measurement. Here the
cw PL measurement is performed by spectrometers coupled
to liquid Nitrogen cooled CCD array (for Visible) or
InGaAs array (for NIR) detectors, and therefore has
superior sensitivity. The TRPL is based on time-correlated
single-photon-counting (TC/SPC) detection mechanism.
An ion-laser pumped cavity-dumped femto-second Ti:S
oscillator (Coherent Mira900D with pulse switch) is
used for pulsed excitation which currently covers NIR
(700nm-1000nm) wavelength range but can be readily adapted
to UV-Vis range (250nm-500nm) via frequency doubling/tripling.
PL generated from sample is spectrally dispersed by
a 1/4m subtractive monochromator and detected by a Hamamatsu
micro-channel plate photomultiplier tube (MCP-PMT) with
S1 cathode covering 400nm-1200nm wavelength range. The
time resolution of this TRPL setup is ~10ps.
A FTIR setup (figure 4)
is also available at NMDL for to perform absorption
and photocurrent measurements of the SAQD arrays and
QDIP device structures in the 1-20 µm
wavelength range. A low temperature cryostat enables
variable temperature absorption and photocurrent measurements
from 1.8 K to room temperature.
Home Labs
& Facilities
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